Facilities
X-Ray Diffraction Lab
Lab Rules
X-Ray Generator
Cryo System
Goniometer Stage
Optical Control
Water Chiller
R-AXIS Overview
R-AXIS Control
R-AXIS Readout
Parts and Accessories
Software
Run/Service Summary
Misc. Procedures
Troubleshooting
Cryo Transfer Stage and Cooling Tube
 

The cryo transfer stage is useful for data collection at very low temperatures. The whole system is composed of a cryo tank that stores liquid nitrogen, a control station, and a cooling tube assemply, of which a nozzle is placed a few millimeters away from a sample on goniometer stage, which is then cooled down to -170oC or lower.
 
 
 
Common Procedures
Filling Up Tank
Cooling
Pumping Tube
Purging Tube
Changing Heater
Aligning Nozzle
Common Problems
Can't Fill Up
Cooling Temp. High
LN From Nozzle
Tube Sweating
Power Trip
Resources
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