Facilities
X-Ray Diffraction Lab
Lab Rules
X-Ray Generator
Cryo System
Goniometer Stage
Optical Control
Water Chiller
R-AXIS Overview
R-AXIS Control
R-AXIS Readout
Parts and Accessories
Software
Run/Service Summary
Misc. Procedures
Troubleshooting
X-Ray Generator
 
The x-ray generator on R-AXIS IIC is composed of two major parts, the rotating anode (target) and the cathode/filament. Both components are housed in an x-ray tube (chamber) under very high vacuum. The target rotates at 6000 rpm, driven by a motor, and cooled by chilled water from a water chiller. The tube is powered up to 50kV and 100mA for data collection. Below is a list of some common procedures and possible problems in the operation/service of the x-ray generator.

 
To service the anode, it's necessary to
1. Undo the belt (see change belt).
2. Release vacuum (see pump/release vacuum).
3. Disconnect water hoses (four of them).
4. Dismount the rotation sensor (see the drawing to the left).
5. Remove side cover [need to undo four (green in the figure) screws], which also removes the whole anode assembly, and cover the side with a replacement plate (which is in one of the tool/accessory drawers in the lab).
6. After service, re-install the assembly in reversed order.
To service the cathode/filament, it's necessary to
1. Release vacuum.
2. Remove front cover [also need to undo four (green in the figure) screws].
3. After service, re-install cathode/filament in reversed order.

 

Common Procedures
X-ray generation
Power-up
Change Belt
Polish Anode
Change Water Seal
Change Filament
Change Megnetic Cassette Seal
Pump Release Vacuum
Common Problems
Can't Get X-Ray
Unable to Power-up
Belt Noise
Dirty Anode
Leaking Water
Fluctuating Current
Anode Noise
Bad Vacuum
Machine Down on Anode Rotation
Resources
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