Facilities
X-Ray Diffraction Lab
Lab Rules
X-Ray Generator
Cryo System
Goniometer Stage
Optical Control
Water Chiller
R-AXIS Overview
R-AXIS Control
R-AXIS Readout
Parts and Accessories
Software
Run/Service Summary
Misc. Procedures
Troubleshooting

Procedure to Check Beam Quality

Even if you get a high beam intensity, it does not necessarily mean that you have a good beam. The final thing is whether you can get good diffraction out of your sample. Mount an alignment crystal, take a shot and compare the diffraction with previous pictures that are considered to be good. The tricky thing is that for quantitive comparison, you have to make sure the crystal is mounted with the same orientation as the last time. This could be troublesome because users of this lab may do the same frequently and everyone does diffrently. However, this should at least tell you whether the beam is bad if you do not get any diffraction at all or what you get is simply too much worse than your expectation. For details, check with R-AXIS Readout

On the other hand, the minimum you can do is to check the direct beam in terms of its intensity and shape.

Common Procedures
Beam Alignment
Collimator Adjustment
Beam Testing
Mirror Box Service
Common Problems
No Beam
Beam Too Weak
Beam Too Strong
Dirty Anode
Leaking Water
Fluctuating Current
Anode Noise
Bad Vacuum
Machine Down on Anode Rotation
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